南方科技大学知识苑(SUSTech KC): GROWTH AND PASSIVATION OF HALIDE PEROVSKITE

题名	GROWTH AND PASSIVATION OF HALIDE PEROVSKITE
姓名	修京伟
姓名拼音	XIU Jingwei
学号	11856015
学位类型	博士
学位专业	Chemistry
导师	何祝兵
导师单位	材料科学与工程系
外机构导师	Peter Raymond Slater
外机构导师单位	伯明翰大学
论文答辩日期	2022-10-17
论文提交日期	2022-11-29
学位授予单位	伯明翰大学
学位授予地点	英国
摘要	The all-inorganic halide perovskite (CsPbI3) holds promise for photovoltaic applications but suffers from a detrimental phase transformation to a non-perovskite phase δ-CsPbI3 at low-temperature. The synthesis and stabilization routes to this and other all-inorganic halide perovskites are still not ideal, requiring uneconomical elimination of humidity, toxic solvent or high-temperature quenching. The all-solid-state synthesis method is a kind of green method to avoid the use of expensive and hazardous solvents. We have studied the influence of inorganic element doping and find that, on the one hand, the incorporation of other metal ions such as Bi³⁺ and Mn²⁺ makes little contribution to the stabilization of CsPbI3; on the other hand, these ions seems to aid the formation of yellow phase at lower temperature and accelerate the decomposition of yellow phase into CsI and PbO at high temperature. Br^- doping is able to stabilize CsPbI3 in air only for a few minutes to an hour, which lead to some observation of cubic phase in the PXRD pattern. Interestingly, a cubic phase dominant black powder can be obtained by the synergic contribution of Br^-and MA⁺/FA⁺ cations. We also studied the synthesis of CsPbI3 in air atmosphere at room temperature by solvent method. Water/moisture is commonly meticulously avoided due the fact that it can accelerate the detrimental degradation of the perovskite. In our work, we used an alternative approach of engineering an in situ degradation process to form a dual-functional PbI(OH) protective covering and succeeded in performing the first room-temperature synthesis of γ-CsPbI3 under ambient humidity. The vastly improved stability benefits from both lattice anchoring and physical coverage of γ-CsPbI3 by an ultra-thin PbI(OH) layer. The resultant γ-CsPbI3 isstable for more than 2 months under ambient conditions (25 ^oC, RH 30 - 60%). Anti-solvent assistanted crystallization (ASAC) is one the most commonly used methods for the deposition of high-quality perovskite solar cells, where anti-solvents are working to modulate the nucleation process of perovskite films by removing the host solvents, such as N,N-Dimethylformamide (DMF), Dimethyl sulfoxide (DMSO), γ-butyrrolactone (GBL). Their toxicity become a concern during the commercialization process of perovskite solar cells. Various green anti-solvents have appeared in recent years, aiming to reduce the hazardouspollution to human and environment during large-scale industrial production. However, limited green solvents, such acetic ether, anisole and so on, are proven to be efficient to reduce the dependence to the widely used toxic chlorobenzene (CB) and toluene (Tol). One of the most essential reasons is that the green anti-solvent couldn’t satisfy the strict requirement of the self-nuclei process in high-quality perovskite films. To overcome this obstacle andestablish more choices for green anti-solvents, we reduce the dependence of perovskite films to self-nuclei process, by adding perovskite CsPbI3 NCs as artificial seeds. When CsPbI3 NCs are added along with the alkane anti-solvents, the NCs could compensate the self-nuclei deficit and result in a high crystalline and dense film for high-efficiency.
关键词	Perovskite Lattice-anchoring Solar Cell Green Chemistry
语种	英语
培养类别	联合培养
入学年份	2018
学位授予年份	2022-12
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推荐引用方式 GB/T 7714	Xiu JW. GROWTH AND PASSIVATION OF HALIDE PEROVSKITE[D]. 英国. 伯明翰大学,2022.

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